The Dow Corning® fluids exhibit outstanding oxidation
resistance at elevated temperatures for a moderate cost. However, it is
generally not recommended that this family of fluids be used in an electron
microscope column for several different reasons:
- If the column should be accidentally flooded with pump fluid (e.g. the
result of a vacuum failure), it is far more difficult to clean up than if
using hydrocarbon fluid.
- If you are doing EDS work, you are very likely from them on to
see a Si peak in all EDS spectra, something not especially attractive should
you have the need also to be making measurements on Si containing samples.
- If using silicone fluids in a vacuum evaporator and you are making carbon
films which will later be analyzed by EDS, it is nearly impossible to obtain
Si-free carbon films under those circumstances. Furthermore, these fluids
should not be used in a mechanical pump which would mean that would be a
basic incompatibility between the fluid in the diffusion pump vs. the fluid
in the mechanical pump.
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