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Apiezon® M and L Ultra High and High Vacuum Greases

Technical information sheet



Introduction

Apiezon L and M greases have been specifically developed for vacuum use, but are also extensively used for non-vacuum purposes in a variety of industrial and scientific applications.

A cross section of the key features of these products are indicated below:



High vacuum

Apiezon L grease has the best vapor pressure properties of all the Apiezon products and can be used in the very high vacuum range, while M grease can be used in high vacuum conditions. Full information on the vapor pressures of both M and L over the working temperature range is shown below. Note that data for a new Apiezon grease is also given. That is called type N. At the present time, it is not a regular SPI products. Should you find it important to have, let us know, we would be happy to process the order for you.



Cryogenic applications

Apiezon N grease has a unique position in the market and is widely recognized and recommended as the cryogenic vacuum grease of choice.

Ambient temperatures

Apiezon L and M and N greases are generally used at ambient temperatures. If you require a grease for use at higher temperatures, Apiezon AP 101 or Apiezon H may be the answer. Or alternatively, the higher use temperatures of the Braycote Micronic 803 grease might be worthy of some consideration.

Silicone free

Being hydrocarbon based, Apiezon greases do not suffer from the problems of "creep" or "carry over" which is traditionally associated with silicone greases.

This benefits scientific users because the risk of sample contamination and consequently the risk of interference in analytical techniques such as infra -red or mass spectrometry, etc. is avoided.

In industrial applications, silicone creeping can create problems in industrial paint or metal deposition processes as trace amounts of silicone on surfaces prevent the adherence of paint and poor or incomplete coverage results.

Trace element analysis:
Such analyses on a lot per lot basis are in general not available. However, some years ago, the trace element analysis for Apiezon L was found to be the following:

Fe      1 ppm
Si      4 ppm
Ti      5 ppm
V      2 ppm

All metals: Pb, Cu, Cr, Al, Ni, Ag, Sn, B, Na, P, Zn, Ca, Ba, Mg, Ti, Mo, V: Less then 1 ppm

We can not guarantee that presently manufactured Apiezon L will give the same trace element analysis results, however in any case, we would expect the impurity levels today to be fairly comparable to what they were in the past. Should the presence of trace elements be a critical issue for one of our customers, then we would suggest that they conduct their own analysis on a tube of Apiezon L.

Radiation resistant

For a radiation resistant grease look no further than Apiezon L or M grease, as both have built-in resistance to radiation. They are markedly better lubricants at higher irradiation levels than other high vacuum greases like silicones, esters or halogenated paraffins, which decompose at radiation levels of 10 Mrads or less.

However, in the electron microscope application, the slow evolution of hydrocarbon organics results in molecular species that will be cross-linked and polymerized in the electron microscope column, contributing to the formation of a layer of contamination or "varnish" on the inside of the column surfaces. Hence in high performance electron microscope applications , the perfluorinated-type systems based on fluorocarbon materials have the advantage since such species, when they evaporate are inert in the presence of radiation and won't polymerize and contribute to column contamination.

Non vacuum applications

Apiezon L and M greases have strong powers of absorption, particularly for other hydrocarbon molecules due to their complex hydrocarbon structure and very high molecular weight. They are frequently used as the stationary phase in gas chromatography.

Long lasting lubrication

Apiezon L and M greases have been especially formulated to provide excellent lubrication while maintaining an efficient gas seal and are widely used in the manufacture and servicing of high performance vacuum pumps.



Industry approvals

Apiezon vacuum greases have gained many prestigious approvals. Apiezon L grease, for example, is approved by the European Space Agency, Matra Marconi , NASA, and NATO, while M grease is approved by NATO, and N grease is approved by NASA and the US Army.

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Thursday February 09, 2012
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